ISO 527-2: Zugversuche für Kunststoffe

The Definitive Guide to Performing ISO 527-2 Tensile Testing on Plastics

Autor: Erica Lawrence

ISO 527-2 ist eine internationale Norm zur Bestimmung der Zugeigenschaften von verstärkten und unverstärkten Kunststoffen. Obwohl sie ähnliche Ergebnisse wie die ASTM D638 liefert, wird die ISO 527-2 aufgrund von Unterschieden in der Probengröße und den Testanforderungen nicht als technisch gleichwertig angesehen. Während einige große multinationale Hersteller sowohl nach ASTM D638 als auch nach ISO 527-2 testen, zeigen die meisten unserer Kunden eine Präferenz für die eine oder andere Norm, basierend auf ihrem geografischen Standort. Nordamerikanische Hersteller testen in der Regel nach ASTM D638, während die Hersteller in Europa und Asien hauptsächlich nach ISO 527-2 testen. Kunden in China testen gleichermaßen nach ASTM D638 und nach ISO 527-2.

Dieser Leitfaden soll Sie in die grundlegenden Elemente eines Kunststoff-Zugversuchs nach ISO 527-2 einführen, sollte aber nicht als adäquater Ersatz für die Lektüre der vollständigen Norm angesehen werden.


ISO 527-2 Zugversuch an Kunststoffen mit Automatisierung und AVE 2


So führen Sie einen Zugversuch an Kunststoffen nach ISO 527-2 durch:

ISO 527-2 wird auf einer Universalprüfmaschine durchgeführt, indem eine Zugkraft auf eine Probe (Probekörper) aufgebracht und verschiedene Eigenschaften des Probenmaterials unter Spannung gemessen werden. Der Test wird mit Zuggeschwindigkeiten von 1 mm/min bis 500 mm/min durchgeführt, bis die Probe versagt (nachgibt oder bricht).



Was misst die ISO 527-2?

Obwohl die ISO 527-2 viele verschiedene Zugeigenschaften misst, sind die Folgenden die häufigsten:

  • Zugfestigkeit: Die Menge an Kraft, die auf ein Material ausgeübt werden kann, bevor es nachgibt (sich irreparabel dehnt) oder bricht.
  • Zugmodul: Wie stark sich ein Material bei Belastung verformen (dehnen) kann, bevor es nachgibt. Der Modulus ist ein Maß für die Steifigkeit des Materials.
  • Dehnung: Die Zunahme der Messlänge nach dem Bruch geteilt durch die ursprüngliche Messlänge. Eine größere Dehnung weist auf eine höhere Duktilität hin.
  • Poisson-Verhältnis: Ein Maß für das Verhältnis zwischen der Dehnung eines Materials und der Dünnheit, die es während des Dehnungsvorgangs annimmt.

Ist ISO 527-2 die richtige Norm für Sie?

Es gibt viele verschiedene Prüfmethoden für verschiedene Kunststoffarten. ISO 527-2 ist für die Prüfung von starren und halbstarren Kunststoffen vorgesehen, unabhängig davon, ob sie geformt, extrudiert, bearbeitet oder gegossen sind. ISO 527-2 gilt auch für verstärkte Kunststoffe (mit Ausnahme von faserverstärkten Kunststoffen, die unter ISO 527-4 und ISO 527-5 behandelt werden). Bei der Prüfung von Folien und Blechen mit einer Dicke von weniger als 1 mm sollte die ISO 527-3 verwendet werden. Diese und weitere Methoden finden Sie in den Anwendungsmodulen von Bluehill® Universal, die vorkonfigurierte Methodenvorlagen für die gängigsten ISO- und ASTM-Normen enthalten.


Auswahlbildschirm für Bluehill Universal-Testmethoden

Zugprüfmaschine

Die meisten Prüfungen nach ISO 527-2 werden auf einer Tisch-Universalprüfmaschine durchgeführt. Ein 5-kN- oder 10-kN-System (1125 lbf oder 2250 lbf) ist am gebräuchlichsten, aber mit zunehmender Festigkeit von verstärkten Kunststoffen und Verbundwerkstoffen können auch Einheiten mit höherer Kapazität wie 30-kN- oder 50-kN-Systeme erforderlich sein.

Die Universalprüfmaschinen der Serien 3400 und 6800 von Instron sind ideal für die Prüfung nach ISO 527-2. Kunden mit hohem Testbedarf, die weltweit tätig sind, und Kunden mit fortgeschrittenen Forschungsanwendungen bevorzugen jedoch in der Regel die Systeme der Serie 6800 mit dem pneumatischen Spannzeug 2712, das zusätzliche Vorteile bei den Genauigkeitsspezifikationen und Effizienzsteigerungen bietet.

ISO 527-2 test setup

ISO 527-2 Test Setup

1. Instron 6800

2. Bluehill Universal Dashboard (2490-696)

3. AVE2 Video Extensometer (2663-902)

4. 2580 Series Load Cell

5. 5 kN Pneumatic Side-Action Grips (2712-045)

 

 

Tensile Grips

Because the testing process subjects specimens to intense forces, it is important that the specimens be held securely inside of the test machine. Side-action pneumatic grips with serrated jaw faces are often the best grips for holding rigid plastics. Pneumatic grips maintain their gripping force with air pressure, which remains constant even if the specimen deforms during testing and its thickness changes significantly. For forces above 10 kN, typically only found with reinforced materials, manual wedge-action grips are preferred.

10 kN Model | 2712-046
5 kN Model | 2716-010

Extensometers

Extensometers are used to gather modulus data, which is one of the most important properties evaluated in ISO 527-2. Modulus of elasticity is the measurement of how much a material stretches or deforms in response to tensile force. Extensometers for measuring modulus must comply with ISO 9513 Class 1 with 1% accuracy, and several options are available depending on the needs of your laboratory. The simplest type is a fixed-gauge length 2630 series clip-on extensometer, which must be clipped directly onto the specimen at the beginning of each test and removed after the specimen yields or before the specimen breaks.

If testing for Poisson’s ratio, a transverse extensometer must also be added to measure the change in width throughout the elastic region of the specimen. A standalone transverse extensometer can be used to supplement an existing clip-on or automatic extensometer, or a biaxial device can be used to measure both axial and transverse strain simultaneously.


Axial and Biaxial Clip-On Extensometers


In labs with high throughput needs, automatic extensometers can help eliminate the time-consuming need for manual manipulation by the operator, and also provide more consistent placement on a large number of specimens, increasing repeatability values. The AutoX750 automatically attaches to the specimen without interference by the test operator. The Advanced Video Extensometer (AVE 2) is a non-contacting extensometer which uses a camera to track deformation of the specimen throughout the test. If testing to other standards, such as ASTM D638 or ISO 178, automatic extensometers also provide the flexibility of using different gauge lengths with a single device.


AutoX750 Automatic Contacting Extensometer and AVE 2 Non-Contacting Video Extensometer for Plastic Tensile Testing


Specimen Types

There are six possible specimen sizes for testing to ISO 527-2. The preferred specimens are dumbbell-shaped specimens types 1A (injection molded) and 1B (machined). While there are differences in length between these two specimen types, they share a nominal width of 10 mm and thickness of 4 mm. The preferred gauge length for Type 1A specimens is 75 mm, which is a change to the standard introduced in 2012. Until 2012, the preferred gauge length for type 1A was 50 mm, which is still acceptable for quality control testing or where specified. 

In instances where material is limited, many labs will use sub-sized specimens of types 1BA, 1BB, 5A, or 5B. In these cases it may be technically difficult to measure modulus because of small gauge lengths and short testing times. Results obtained from small specimens are not comparable with those obtained from type 1 specimens.

ISO 527-2 Plastic Testing Samples

Specimen Measurement

All specimens must be measured before testing in accordance with ISO 16012 or ISO 23529. Most typical micrometers should be suitable for performing these measurements. In order for the test system to display Stress measurements rather than just Force measurements, operators will be asked to input the cross-sectional area (thickness and width) of the specimen, because Stress = Force / Cross-Sectional Area (this is shown in units of Psi, Pa, kPa, GPa, etc). While the thickness and width of rigid specimens require different measurement accuracies, it is common to use the same measuring device for both. Either cylindrical or rectangular tips can be used, assuming they meet the dimensional requirements provided by ISO 16012. Injection molded specimens are often produced with a draft angle instead of being perfectly square, so care must be taken to measure width at the center of the draft angle.


Bluehill Universal Specimen Dimensions


Specimen Loading

In order to obtain proper results, specimens must be correctly aligned inside the grips. One way of preventing misalignment is by using a jaw face that is close to the same width as the specimen, making it easier to visually adjust the alignment. The simplest way to prevent misalignment is to use a specimen alignment device which mounts directly onto the grip bodies.

Once the grips tighten onto a specimen, unwanted compressive forces are usually applied. These forces, although minute, can interfere with test results if not treated properly: It is important that they not be balanced after the specimen is inserted, as this will cause an offset in results. Bluehill Universal software can be programmed to normalize forces across multiple specimens and remove any slack or compressive force, ensuring consistent results between specimens. On the 5900 Series universal testing machines we also recommend the use of Specimen Protect, which is designed to prevent damage to the specimen or system during the setup phase of a test, before a test’s operational limits are defined. When turned on, Specimen Protect automatically adjusts the crosshead to keep any unwanted forces under a certain limit. 


Calculations and Results

When presenting test results, it is important to ensure that the terms are properly defined in order to comply with the ISO standard and facilitate data comparison between different laboratories.


Strain Measurement

The most common mistake in data reporting is the reporting of strain values using an incorrect source. For plastics, percent elongation at break often cannot be measured exclusively by an extensometer because plastic does not break down homogenously and strain is often focused on a disproportionately small part of the sample, a property known as "necking." Because necking may occur outside of the extensometer's gauge length, a term called "nominal strain" must be used to report percent elongation at any points after yield. Using an extensometer for strain at break is only acceptable if the strain is homogenous throughout the specimen and does not exhibit necking or yield.

Nominal strain is defined differently depending on which test method is being used. For ISO 527-2, nominal strain can be measured in two different ways: Method A measures nominal strain purely by crosshead displacement, but for multipurpose specimens, Method B is preferred. Method B measures nominal strain as the strain measured from the extensometer until yield and and from crosshead displacement after yield, which ensures that necking behavior outside of the extensometer gauge length is taken into account.


Modulus

ISO 527-2 defines modulus as the slope of the curve between 0.05% and 0.25% strain using either a chord or a linear regression slope calculation. Because the modulus calculation starts at 0.05% strain, it is extremely important that appropriate pre-stresses are applied to the material to remove any slack or compressive forces induced from gripping the specimen. It shall not exceed 0.05% strain or 1% of the tensile strength of the material.


Tensile Strength

In the 2012 update to the standard, a change was made to the definition of tensile strength. In previous versions, tensile strength was defined as the maximum stress at any time throughout the test. In the latest version of ISO 527-2, tensile strength is taken at the first local maximum exhibited. This change is particularly critical for customers testing materials which have yield points such as polypropylene, polyethylene, and nylons. 

Tensile Strength Graph

Throughput

For labs with high-volume testing needs, several modifications to the tensile machine setup can be made to speed up the testing process and increase throughput, up to and including fully automated test systems. Fully automated systems are designed to incorporate specimen measurement, specimen loading, testing, and removal, and are able to run for hours without operator interaction. These systems help to reduce variability due to human error and can be left running after a shift ends to continue getting results when operators go home.

 

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